6ZI3
Crystal structure of OleP-6DEB bound to L-rhamnose
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ELETTRA BEAMLINE 11.2C |
Synchrotron site | ELETTRA |
Beamline | 11.2C |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2019-05-16 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 1.00 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 247.379, 111.149, 159.144 |
Unit cell angles | 90.00, 129.40, 90.00 |
Refinement procedure
Resolution | 48.090 - 2.080 |
R-factor | 0.17438 |
Rwork | 0.172 |
R-free | 0.22501 |
Structure solution method | FOURIER SYNTHESIS |
Starting model (for MR) | 5mns |
RMSD bond length | 0.011 |
RMSD bond angle | 1.754 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | REFMAC |
Refinement software | REFMAC (5.8.0238) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.080 |
High resolution limit [Å] | 1.960 | 1.960 |
Rmerge | 0.064 | 1.640 |
Number of reflections | 462663 | 73872 |
<I/σ(I)> | 7.8 | |
Completeness [%] | 97.7 | |
Redundancy | 2.7 | |
CC(1/2) | 0.997 | 0.362 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 294 | 4.2 M Sodium Formate (HCOONa) |