6Z9Y
Copper transporter OprC
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I24 |
Synchrotron site | Diamond |
Beamline | I24 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2019-11-23 |
Detector | DECTRIS PILATUS3 6M |
Wavelength(s) | 1.40889 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 67.341, 197.668, 171.749 |
Unit cell angles | 90.00, 88.75, 90.00 |
Refinement procedure
Resolution | 85.850 - 2.950 |
R-factor | 0.2451 |
Rwork | 0.242 |
R-free | 0.30220 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 6fok |
RMSD bond length | 0.009 |
RMSD bond angle | 1.163 |
Data reduction software | xia2 |
Data scaling software | Aimless |
Phasing software | PHENIX |
Refinement software | PHENIX (1.18_3855) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 197.670 | 3.000 |
High resolution limit [Å] | 2.950 | 2.950 |
Rpim | 0.081 | |
Number of reflections | 94129 | 9369 |
<I/σ(I)> | 5.56 | |
Completeness [%] | 100.0 | |
Redundancy | 6.6 | |
CC(1/2) | 0.551 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 5.5 | 293 | 0.34 M Ammonium sulfate 0.1 M Sodium citrate 12 -16 % w/v PEG 4000 2 mM CuSO4 |