6Z8S
Copper transporter OprC
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I03 |
Synchrotron site | Diamond |
Beamline | I03 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2020-02-09 |
Detector | DECTRIS EIGER2 XE 16M |
Wavelength(s) | 1.351326 |
Spacegroup name | C 2 2 21 |
Unit cell lengths | 156.100, 195.690, 166.650 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 61.020 - 2.370 |
R-factor | 0.2203 |
Rwork | 0.219 |
R-free | 0.25170 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 6fok |
RMSD bond length | 0.008 |
RMSD bond angle | 0.988 |
Data reduction software | xia2 |
Data scaling software | Aimless |
Phasing software | PHENIX |
Refinement software | PHENIX (1.18_3855) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 97.850 | 2.410 |
High resolution limit [Å] | 2.370 | 2.370 |
Rpim | 0.044 | |
Number of reflections | 103185 | 10239 |
<I/σ(I)> | 12.46 | |
Completeness [%] | 100.0 | |
Redundancy | 13.27 | |
CC(1/2) | 0.315 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6.5 | 293 | 0.1 M NaCl 0.15 M NH4SO4 0.1 M MES 18-22% PEG1000 3 mM CuSO4 |