Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SLS BEAMLINE X06SA |
| Synchrotron site | SLS |
| Beamline | X06SA |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2018-11-11 |
| Detector | DECTRIS EIGER X 16M |
| Wavelength(s) | 1.000031 |
| Spacegroup name | C 2 2 21 |
| Unit cell lengths | 76.186, 212.992, 94.639 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 29.461 - 3.192 |
| Rwork | 0.286 |
| R-free | 0.29430 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 6yvr |
| RMSD bond length | 0.002 |
| RMSD bond angle | 1.196 |
| Data reduction software | XDS |
| Data scaling software | Aimless |
| Phasing software | PHASER |
| Refinement software | REFMAC (5.8.0258) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 29.461 | 3.435 |
| High resolution limit [Å] | 3.192 | 3.192 |
| Rmerge | 0.330 | 3.661 |
| Rmeas | 0.344 | 3.807 |
| Rpim | 0.094 | 1.034 |
| Number of reflections | 10818 | 541 |
| <I/σ(I)> | 7.7 | 1.3 |
| Completeness [%] | 91.6 | |
| Redundancy | 13.3 | |
| CC(1/2) | 0.993 | 0.316 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | LIPIDIC CUBIC PHASE | 4.5 | 293.1 | 100 mM Na acetate 400-475 mM K citrate 30-31% (v/v) PEG400 |
