6Z3K
Structure of protective antibody 38-1-10A Fab
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I03 |
Synchrotron site | Diamond |
Beamline | I03 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2018-05-17 |
Detector | DECTRIS PILATUS3 6M |
Wavelength(s) | 0.9763 |
Spacegroup name | P 21 21 2 |
Unit cell lengths | 292.350, 87.130, 177.030 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 65.520 - 2.700 |
R-factor | 0.1905 |
Rwork | 0.188 |
R-free | 0.23430 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3dgg |
RMSD bond length | 0.004 |
RMSD bond angle | 0.745 |
Data reduction software | xia2 |
Data scaling software | xia2 |
Phasing software | PHASER |
Refinement software | PHENIX (dev_3699) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 67.500 | 2.750 |
High resolution limit [Å] | 2.700 | 2.700 |
Rmerge | 0.370 | |
Number of reflections | 124934 | 6090 |
<I/σ(I)> | 16.4 | 1.1 |
Completeness [%] | 100.0 | |
Redundancy | 53.8 | |
CC(1/2) | 1.000 | 0.600 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 4 | 293 | 20% (v/v) PEG 6000, 0.1 M citrate, pH 4.0, 1 M lithium chloride |