6Z3D
L-FerritinMSA
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID23-1 |
Synchrotron site | ESRF |
Beamline | ID23-1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2017-06-29 |
Detector | DECTRIS PILATUS 6M-F |
Wavelength(s) | 0.977999 |
Spacegroup name | P 4 21 2 |
Unit cell lengths | 134.297, 134.297, 166.853 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 166.850 - 1.700 |
R-factor | 0.1561 |
Rwork | 0.155 |
R-free | 0.17590 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1lb3 |
RMSD bond length | 0.013 |
RMSD bond angle | 1.670 |
Data reduction software | XDS |
Data scaling software | Aimless (0.5.32) |
Refinement software | REFMAC (5.8.0238) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 166.850 | 1.730 |
High resolution limit [Å] | 1.700 | 1.700 |
Rmerge | 0.225 | 4.065 |
Rmeas | 0.230 | 4.145 |
Rpim | 0.044 | 0.805 |
Number of reflections | 166767 | 8116 |
<I/σ(I)> | 14.4 | |
Completeness [%] | 100.0 | 100 |
Redundancy | 26.5 | 26.5 |
CC(1/2) | 0.999 | 0.606 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 8 | 293 | 0.1 M sodium acetate pH 4.6 and 2 M sodium formate |