Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | DIAMOND BEAMLINE I02 |
| Synchrotron site | Diamond |
| Beamline | I02 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2013-12-02 |
| Detector | DECTRIS PILATUS 6M |
| Wavelength(s) | 0.9795 |
| Spacegroup name | P 41 |
| Unit cell lengths | 84.500, 84.500, 118.720 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 84.640 - 2.310 |
| R-factor | 0.20017 |
| Rwork | 0.197 |
| R-free | 0.25614 |
| Structure solution method | FOURIER SYNTHESIS |
| Starting model (for MR) | 4idt |
| Data reduction software | xia2 |
| Data scaling software | xia2 |
| Phasing software | REFMAC |
| Refinement software | REFMAC (5.8.0258) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 84.643 | 2.370 |
| High resolution limit [Å] | 2.310 | 2.310 |
| Rmeas | 0.091 | 0.689 |
| Number of reflections | 36568 | 2685 |
| <I/σ(I)> | 15.5 | 2.4 |
| Completeness [%] | 100.0 | |
| Redundancy | 6.5 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION | 7.6 | 277 | 12-20% Ethanol, 0.1M Hepes pH 7.6 |
