Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | DIAMOND BEAMLINE I04 |
| Synchrotron site | Diamond |
| Beamline | I04 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2013-10-05 |
| Detector | DECTRIS PILATUS 6M-F |
| Wavelength(s) | 0.9795 |
| Spacegroup name | P 41 |
| Unit cell lengths | 84.770, 84.770, 118.520 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 68.950 - 2.420 |
| R-factor | 0.19301 |
| Rwork | 0.190 |
| R-free | 0.24588 |
| Structure solution method | FOURIER SYNTHESIS |
| Starting model (for MR) | 4idt |
| Data reduction software | xia2 |
| Data scaling software | xia2 |
| Phasing software | REFMAC |
| Refinement software | REFMAC (5.8.0258) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 68.950 | 2.480 |
| High resolution limit [Å] | 2.420 | 2.420 |
| Rmeas | 0.059 | 0.663 |
| Number of reflections | 31830 | 2366 |
| <I/σ(I)> | 19.3 | 2.3 |
| Completeness [%] | 99.6 | |
| Redundancy | 4.4 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION | 7.6 | 277 | 12-20% Ethanol, 0.1M Hepes pH 7.6 |
