6Z1D
Crystal structure of the AAA domain of Rubisco Activase from Nostoc sp. (strain PCC 7120), Gadolinium complex
Experimental procedure
Experimental method | MAD |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06DA |
Synchrotron site | SLS |
Beamline | X06DA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2013-02-09 |
Detector | DECTRIS PILATUS 2M |
Wavelength(s) | 1.68745 |
Spacegroup name | H 3 2 |
Unit cell lengths | 111.990, 111.990, 283.818 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 28.633 - 2.705 |
R-factor | 0.2179 |
Rwork | 0.216 |
R-free | 0.25850 |
Structure solution method | MAD |
RMSD bond length | 0.008 |
RMSD bond angle | 1.098 |
Data reduction software | XDS (VERSION September 26, 2012) |
Data scaling software | SCALA (3.3.16) |
Phasing software | SHELXDE (Version 2006/3) |
Refinement software | PHENIX (1.8.2) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 48.990 | 48.990 | 2.850 |
High resolution limit [Å] | 2.705 | 8.550 | 2.705 |
Rmerge | 0.017 | 0.624 | |
Rmeas | 0.069 | 0.022 | 0.658 |
Rpim | 0.015 | 0.005 | 0.148 |
Total number of observations | 375979 | ||
Number of reflections | 19125 | 674 | 2738 |
<I/σ(I)> | 37.2 | 35 | 1.3 |
Completeness [%] | 99.9 | 99.6 | 99.5 |
Redundancy | 19.7 | 19.3 | 19.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 7 | 277 | 2.2 M Na-acetate |