6YMU
Imidazole Glycerol Phosphate Synthase
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06DA |
Synchrotron site | SLS |
Beamline | X06DA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2018-09-18 |
Detector | DECTRIS PILATUS 300K |
Wavelength(s) | 1 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 80.417, 85.901, 128.745 |
Unit cell angles | 90.00, 108.24, 90.00 |
Refinement procedure
Resolution | 40.000 - 2.110 |
Rwork | 0.210 |
R-free | 0.25000 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1gpw |
RMSD bond length | 0.009 |
RMSD bond angle | 1.057 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | PHENIX (1.17) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 40.000 | 2.180 |
High resolution limit [Å] | 2.110 | 2.110 |
Rmerge | 1.500 | |
Number of reflections | 95686 | 9472 |
<I/σ(I)> | 14 | |
Completeness [%] | 99.0 | |
Redundancy | 6.9 | |
CC(1/2) | 0.990 | 0.550 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 295 | PEG |