6YMC
26-mer stem-loop RNA
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06SA |
Synchrotron site | SLS |
Beamline | X06SA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2015-04-18 |
Detector | DECTRIS PILATUS 2M |
Wavelength(s) | 1.0 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 24.270, 52.430, 107.180 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 50.000 - 2.000 |
R-factor | 0.1784 |
Rwork | 0.175 |
R-free | 0.24090 |
Structure solution method | SAD |
RMSD bond length | 0.013 |
RMSD bond angle | 2.278 |
Data reduction software | XDS |
Data scaling software | SCALA |
Phasing software | Auto-Rickshaw |
Refinement software | REFMAC (5.8.0131) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.010 | 2.050 |
High resolution limit [Å] | 2.000 | 2.000 |
Number of reflections | 9048 | 750 |
<I/σ(I)> | 13.1 | 3.49 |
Completeness [%] | 99.9 | 96 |
Redundancy | 5.9 | 5.7 |
CC(1/2) | 0.987 | 0.681 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7 | 292 | 100 mM NaCl, 15 mM BaCl2, 40 mM Na Cacodylate 7.0 44 % MPD, 12 mM spermine tetrahydrochloride |