6YDF
X-ray structure of LPMO.
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ESRF BEAMLINE MASSIF-3 |
| Synchrotron site | ESRF |
| Beamline | MASSIF-3 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2017-02-18 |
| Detector | DECTRIS EIGER X 4M |
| Wavelength(s) | 0.96 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 51.120, 39.390, 119.930 |
| Unit cell angles | 90.00, 93.78, 90.00 |
Refinement procedure
| Resolution | 50.000 - 2.120 |
| R-factor | 0.19979 |
| Rwork | 0.197 |
| R-free | 0.24944 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 5ach |
| Data reduction software | XDS |
| Data scaling software | XSCALE |
| Phasing software | MOLREP |
| Refinement software | REFMAC (v5.8.0230) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 50.000 | 2.180 |
| High resolution limit [Å] | 2.120 | 2.120 |
| Number of reflections | 26050 | 1853 |
| <I/σ(I)> | 8.7 | |
| Completeness [%] | 94.5 | |
| Redundancy | 4.02 | |
| CC(1/2) | 0.995 | 0.508 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 298.15 | 0.1 M NaCl, 0.1 M HEPES pH 6.5, 1.5 M (NH4)2SO4 |
