6YDD
X-ray structure of LPMO.
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE MASSIF-3 |
Synchrotron site | ESRF |
Beamline | MASSIF-3 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2017-04-27 |
Detector | DECTRIS EIGER X 4M |
Wavelength(s) | 0.90 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 52.140, 39.700, 120.650 |
Unit cell angles | 90.00, 93.49, 90.00 |
Refinement procedure
Resolution | 2.870 - 2.800 |
R-factor | 0.20073 |
Rwork | 0.198 |
R-free | 0.26087 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5ach |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | MOLREP |
Refinement software | REFMAC (v5.8.0230) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.870 |
High resolution limit [Å] | 2.800 | 2.800 |
Number of reflections | 12356 | 924 |
<I/σ(I)> | 5.82 | 1.08 |
Completeness [%] | 98.2 | 99.1 |
Redundancy | 5.51 | 2.96 |
CC(1/2) | 0.969 | 0.547 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 298.15 | 0.1 M NaCl, 0.1 M Bis-Tris pH 6.5, 2.0 M (NH4)2SO4 |