6YDC
X-ray structure of LPMO
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE MASSIF-3 |
Synchrotron site | ESRF |
Beamline | MASSIF-3 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2017-02-18 |
Detector | DECTRIS EIGER X 4M |
Wavelength(s) | 0.96 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 39.790, 120.800, 136.360 |
Unit cell angles | 90.00, 92.09, 90.00 |
Refinement procedure
Resolution | 50.000 - 2.000 |
R-factor | 0.21695 |
Rwork | 0.215 |
R-free | 0.26209 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5ach |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | MOLREP |
Refinement software | REFMAC (v5.8.0230) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.050 |
High resolution limit [Å] | 2.000 | 2.000 |
Number of reflections | 85419 | 6184 |
<I/σ(I)> | 5.54 | 1.44 |
Completeness [%] | 98.4 | 97.2 |
Redundancy | 4.55 | 4.16 |
CC(1/2) | 0.989 | 0.544 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 6.5 | 298.15 | 0.1 M NaCl, 0.1 M HEPES pH 6.5, 1.5 M (NH4)2SO4 |