6YBE
RNASE 3/1 version2
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ALBA BEAMLINE XALOC |
Synchrotron site | ALBA |
Beamline | XALOC |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2019-06-15 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.9792568 |
Spacegroup name | I 1 2 1 |
Unit cell lengths | 43.210, 61.770, 51.346 |
Unit cell angles | 90.00, 106.88, 90.00 |
Refinement procedure
Resolution | 38.450 - 1.140 |
R-factor | 0.152 |
Rwork | 0.151 |
R-free | 0.16550 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2k11 |
RMSD bond length | 0.007 |
RMSD bond angle | 1.010 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | PHENIX (1.15.2_3472) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 38.450 | 1.140 |
High resolution limit [Å] | 1.120 | 1.120 |
Number of reflections | 43663 | 2247 |
<I/σ(I)> | 16.9 | |
Completeness [%] | 92.6 | 90.9 |
Redundancy | 2.1 | |
CC(1/2) | 0.996 | 0.966 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 293 | 100 mM sodium acetate pH 5 and 1 M sodium chloride |