6Y2D
Crystal structure of the second KH domain of FUBP1
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06SA |
Synchrotron site | SLS |
Beamline | X06SA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2018-04-19 |
Detector | DECTRIS EIGER X 16M |
Wavelength(s) | 0.9998 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 28.888, 82.181, 49.371 |
Unit cell angles | 90.00, 91.04, 90.00 |
Refinement procedure
Resolution | 49.360 - 1.900 |
R-factor | 0.1978 |
Rwork | 0.195 |
R-free | 0.23950 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4lij |
RMSD bond length | 0.016 |
RMSD bond angle | 1.684 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0258) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 49.400 | 1.940 |
High resolution limit [Å] | 1.900 | 1.900 |
Number of reflections | 18030 | 1152 |
<I/σ(I)> | 5.3 | |
Completeness [%] | 99.0 | |
Redundancy | 3.9 | |
CC(1/2) | 0.990 | 0.719 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 293 | 2M ammonium sulfate, 5% 2-propanol, 2.5% Glycerol |