6V8A
Human CtBP1 (28-375) in complex with AMP
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | Cu FINE FOCUS |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2019-07-03 |
Detector | RIGAKU SATURN 944 |
Wavelength(s) | 1.54178 |
Spacegroup name | P 64 2 2 |
Unit cell lengths | 89.171, 89.171, 164.170 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 31.550 - 2.350 |
R-factor | 0.2052 |
Rwork | 0.203 |
R-free | 0.25790 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 6cdf |
RMSD bond length | 0.002 |
RMSD bond angle | 0.459 |
Data reduction software | HKL-3000 |
Data scaling software | HKL-2000 |
Phasing software | PHASER |
Refinement software | PHENIX (v1.15) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 50.000 | 50.000 | 2.390 |
High resolution limit [Å] | 2.350 | 6.370 | 2.350 |
Rmerge | 0.107 | 0.039 | 0.985 |
Total number of observations | 157772 | ||
Number of reflections | 16758 | 959 | 771 |
<I/σ(I)> | 6.4 | ||
Completeness [%] | 99.7 | 97.9 | 96 |
Redundancy | 9.4 | 11.2 | 3.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.5 | 298 | 100 mM HEPES, pH 7.5, 80-200 mM calcium chloride, 2-6% PEG400 |