6UYZ
Crystal structure of K46-acetylated SUMO1 in complex with phosphorylated DAXX
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | CLSI BEAMLINE 08ID-1 |
Synchrotron site | CLSI |
Beamline | 08ID-1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2017-06-13 |
Detector | DECTRIS PILATUS3 S 6M |
Wavelength(s) | 0.9795 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 100.224, 38.316, 67.721 |
Unit cell angles | 90.00, 119.91, 90.00 |
Refinement procedure
Resolution | 48.280 - 1.400 |
R-factor | 0.16 |
Rwork | 0.159 |
R-free | 0.18100 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4wjn |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHASER |
Refinement software | PHENIX (1.14-3260_1496) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 48.275 | 1.450 |
High resolution limit [Å] | 1.400 | 1.400 |
Number of reflections | 41097 | 2602 |
<I/σ(I)> | 10.93 | |
Completeness [%] | 92.8 | |
Redundancy | 3 | |
CC(1/2) | 0.997 | 0.428 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 298 | 100MM SODIUM CACODYLATE PH6.5, 26% PEG3350, 10MM CALCIUM CHLORIDE |