6U9J
Crystal structure of ChuX
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 22-ID |
Synchrotron site | APS |
Beamline | 22-ID |
Temperature [K] | 291 |
Detector technology | PIXEL |
Collection date | 2018-02-11 |
Detector | DECTRIS EIGER X 16M |
Wavelength(s) | 0.98 |
Spacegroup name | P 32 |
Unit cell lengths | 50.566, 50.566, 208.969 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 33.560 - 1.500 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2ovi |
Data reduction software | HKL-3000 |
Data scaling software | HKL-3000 |
Phasing software | PHENIX |
Refinement software | PHENIX ((1.12_2829: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 1.550 |
High resolution limit [Å] | 1.500 | 1.500 |
Number of reflections | 95633 | 8000 |
<I/σ(I)> | 36.6 | |
Completeness [%] | 97.3 | |
Redundancy | 13.3 | |
CC(1/2) | 0.999 | 0.995 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | COUNTER-DIFFUSION | 293 | 0.2 M lithium sulfate monohydrate, 20% w/v PEG3350 |