6TUA
The RYK Pseudokinase Domain
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06SA |
Synchrotron site | SLS |
Beamline | X06SA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2018-12-07 |
Detector | PSI PILATUS 6M |
Wavelength(s) | 0.99999 |
Spacegroup name | I 1 2 1 |
Unit cell lengths | 60.645, 47.242, 152.741 |
Unit cell angles | 90.00, 97.64, 90.00 |
Refinement procedure
Resolution | 37.850 - 2.380 |
R-factor | 0.1966 |
Rwork | 0.194 |
R-free | 0.24760 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5tc0 |
RMSD bond length | 0.008 |
RMSD bond angle | 0.879 |
Data reduction software | xia2 |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | PHENIX (1.17.1_3660) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 37.850 | 2.470 |
High resolution limit [Å] | 2.380 | 2.380 |
Number of reflections | 17214 | 1718 |
<I/σ(I)> | 8.3 | 2 |
Completeness [%] | 98.6 | 97 |
Redundancy | 3.7 | |
CC(1/2) | 1.000 | 0.900 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 293 | 1.5 M lithium sulfate, 0.1 M HEPES 7.5 |