6TPR
PqsR (MvfR) bound to inhibitory compound 40
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I04-1 |
Synchrotron site | Diamond |
Beamline | I04-1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2018-10-21 |
Detector | DECTRIS PILATUS 6M-F |
Wavelength(s) | 0.9159 |
Spacegroup name | P 65 2 2 |
Unit cell lengths | 118.754, 118.754, 115.242 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 115.242 | 3.420 |
High resolution limit [Å] | 3.200 | 3.200 |
Rmerge | 0.234 | 1.392 |
Number of reflections | 8390 | 1466 |
<I/σ(I)> | 6.6 | |
Completeness [%] | 99.9 | 99.7 |
Redundancy | 13.5 | 14 |
CC(1/2) | 0.980 | 0.982 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 6 | 293 | 100 mM Sodium citrate, 200 mM Ammonium acetate, 3% (v/v) MPD |