6TL9
CRYSTAL STRUCTURE OF LECTIN-LIKE OX-LDL RECEPTOR 1 IN COMPLEX WITH BI-0115
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SLS BEAMLINE X06SA |
| Synchrotron site | SLS |
| Beamline | X06SA |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2011-07-07 |
| Detector | DECTRIS PILATUS3 6M |
| Wavelength(s) | 1.000000 |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 150.816, 62.211, 116.331 |
| Unit cell angles | 90.00, 93.99, 90.00 |
Refinement procedure
| Resolution | 39.000 - 2.734 |
| R-factor | 0.2231 |
| Rwork | 0.222 |
| R-free | 0.24640 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 1ypu |
| RMSD bond length | 0.006 |
| RMSD bond angle | 0.750 |
| Data reduction software | autoPROC |
| Data scaling software | autoPROC (1.1.6) |
| Phasing software | MOLREP |
| Refinement software | BUSTER (2.11.7 (3-OCT-2019)) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 75.225 | 2.743 |
| High resolution limit [Å] | 2.734 | 2.734 |
| Rmerge | 0.066 | 0.321 |
| Rmeas | 0.084 | 0.388 |
| Rpim | 0.046 | 0.216 |
| Number of reflections | 27991 | 305 |
| <I/σ(I)> | 12.5 | 3.5 |
| Completeness [%] | 97.1 | 97.4 |
| Redundancy | 3.2 | 3.2 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 277 | 0.1 M Bis-Tris pH 7.5, 30% PEG MME 2000 and 0.15 M KBr |
