6TL1

Crystal structure of the TASOR pseudo-PARP domain

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	DIAMOND BEAMLINE I02
Synchrotron site	Diamond
Beamline	I02
Temperature [K]	100
Detector technology	PIXEL
Collection date	2016-03-05
Detector	DECTRIS PILATUS 6M
Wavelength(s)	0.97949
Spacegroup name	P 41 21 2
Unit cell lengths	74.590, 74.590, 184.040
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	57.940 - 2.030
R-factor	0.197
Rwork	0.195
R-free	0.22900
Structure solution method	SAD
Data reduction software	XDS (Oct 15, 2015)
Data scaling software	Aimless (0.5.17)
Phasing software	AutoSol
Refinement software	PHENIX (1.10.1_2155)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	57.945	2.080
High resolution limit [Å]	2.030	2.030
Rmerge	0.094	1.460
Rpim	0.028	0.427
Number of reflections	34589	2513
<I/σ(I)>	16.1
Completeness [%]	100.0	100
Redundancy	12.7	12.6

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, SITTING DROP	6.5	291	0.1 M MES pH 6.5, 0.1 M NaPi,, 0.1 M KPi, 2 M NaCl
1	VAPOR DIFFUSION, SITTING DROP	6.5	291	0.1 M MES pH 6.5, 0.1 M NaPi,, 0.1 M KPi, 2 M NaCl