6TCU
Glycogen synthase kinase-3 beta (GSK3b) in complex with ligand 1
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X10SA |
Synchrotron site | SLS |
Beamline | X10SA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2019-09-29 |
Detector | DECTRIS EIGER X 16M |
Wavelength(s) | 1.00004527943 |
Spacegroup name | C 2 2 21 |
Unit cell lengths | 84.783, 107.851, 104.226 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 66.650 - 2.140 |
R-factor | 0.204 |
Rwork | 0.202 |
R-free | 0.23970 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | NONE |
RMSD bond length | 0.011 |
RMSD bond angle | 1.497 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0155) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 66.650 | 2.390 |
High resolution limit [Å] | 2.140 | 2.140 |
Rmerge | 0.035 | 0.443 |
Number of reflections | 26305 | 7373 |
<I/σ(I)> | 20.08 | 3.52 |
Completeness [%] | 98.5 | 99.3 |
Redundancy | 4.3 | 4.3 |
CC(1/2) | 1.000 | 0.999 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 277 | 18% (w/v) PEG8000 0.13 M NaCl 0.1 M Tris Acetate pH 8.0 |