6TBN
Crystal structure of CIAO1-CIAO2B CIA core complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06DA |
Synchrotron site | SLS |
Beamline | X06DA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2016-04-07 |
Detector | DECTRIS PILATUS 2M |
Wavelength(s) | 1.0000 |
Spacegroup name | I 4 |
Unit cell lengths | 125.580, 125.580, 85.490 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 19.860 - 2.000 |
R-factor | 0.1819 |
Rwork | 0.180 |
R-free | 0.20840 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3fm0 |
RMSD bond length | 0.006 |
RMSD bond angle | 0.704 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | PHASER |
Refinement software | PHENIX (1.16_3549) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 19.860 | 2.071 |
High resolution limit [Å] | 2.000 | 2.000 |
Number of reflections | 44669 | 4240 |
<I/σ(I)> | 14.8 | 0.72 |
Completeness [%] | 99.4 | |
Redundancy | 53.9 | |
CC(1/2) | 0.998 | 0.142 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 293 | 0.1 M Tris pH 8.5, 25% PEG MME 2k |