6TB2
Structure of human haptoglobin-hemoglobin bound to S. aureus IsdH
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PETRA III, EMBL c/o DESY BEAMLINE P13 (MX1) |
Synchrotron site | PETRA III, EMBL c/o DESY |
Beamline | P13 (MX1) |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2018-04-19 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 1.0 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 84.100, 86.770, 217.950 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 78.460 | 3.000 |
High resolution limit [Å] | 2.900 | 2.900 |
Rmeas | 0.084 | 2.960 |
Number of reflections | 35967 | 3445 |
<I/σ(I)> | 15.12 | |
Completeness [%] | 100.0 | |
Redundancy | 12.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 277 | 0.2 M sodium citrate tribasic dihydrate, 20 % w/v PEG 3350 |