6T6Q
Crystal structure of Toxoplasma gondii Morn1 (extended conformation).
This is a non-PDB format compatible entry.
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ESRF BEAMLINE ID30B |
| Synchrotron site | ESRF |
| Beamline | ID30B |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2017-03-03 |
| Detector | DECTRIS PILATUS3 6M |
| Wavelength(s) | 0.967 |
| Spacegroup name | P 43 21 2 |
| Unit cell lengths | 53.916, 53.916, 348.849 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 48.920 - 2.902 |
| Rwork | 0.276 |
| R-free | 0.31110 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 6t4d |
| RMSD bond length | 0.002 |
| RMSD bond angle | 1.213 |
| Data reduction software | XDS |
| Data scaling software | Aimless |
| Phasing software | PHASER |
| Refinement software | REFMAC (5.8.0257) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 48.920 | 3.080 |
| High resolution limit [Å] | 2.900 | 2.900 |
| Rmerge | 0.140 | 2.252 |
| Number of reflections | 12331 | 1819 |
| <I/σ(I)> | 11.8 | 0.5 |
| Completeness [%] | 99.1 | |
| Redundancy | 8.4 | 8 |
| CC(1/2) | 0.992 | 0.772 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 295.15 | 0.1 M Tris-HCl pH 8.2, 15% PEG 3350, 0.2 M NaCl |
