6T6E
Crystal Structure of the C-terminal domain of the HIV-1 Integrase (PNL4-3)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06DA |
Synchrotron site | SLS |
Beamline | X06DA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2017-02-20 |
Detector | DECTRIS PILATUS 2M |
Wavelength(s) | 1.0 |
Spacegroup name | P 63 |
Unit cell lengths | 49.472, 49.472, 39.811 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 42.844 | 1.350 |
High resolution limit [Å] | 1.300 | 1.300 |
Rmerge | 0.059 | 4.151 |
Number of reflections | 13357 | 1227 |
<I/σ(I)> | 254580 | |
Completeness [%] | 99.1 | |
Redundancy | 18.6 | |
CC(1/2) | 1.000 | 0.249 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 293 | 0.1 M Tris pH 7, 0.8 M potassium sodium tartrate and 0.2 M lithium sulfate |