6T6C
Complex with chitin oligomer of C-type lysozyme from the upper gastrointestinal tract of Opisthocomus hoatzin
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I04 |
Synchrotron site | Diamond |
Beamline | I04 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2012-09-16 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 0.9795 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 37.051, 55.008, 65.829 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 42.247 - 1.250 |
Rwork | 0.108 |
R-free | 0.13430 |
Structure solution method | FOURIER SYNTHESIS |
Starting model (for MR) | 6t5s |
RMSD bond length | 0.018 |
RMSD bond angle | 2.191 |
Data reduction software | MOSFLM |
Data scaling software | Aimless |
Refinement software | REFMAC (5.8.0257) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 42.247 | 1.270 |
High resolution limit [Å] | 1.250 | 1.250 |
Rmerge | 0.105 | 0.882 |
Number of reflections | 38043 | 1893 |
<I/σ(I)> | 13.4 | |
Completeness [%] | 99.9 | |
Redundancy | 8 | |
CC(1/2) | 0.998 | 0.535 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 3.5 | 293 | 0.1 M Citric acid pH 3.5, 3.0 M Sodium chloride, Hampton research INDEX screen no 7. |