6T5L
MYO-1 from Myroides odoratimimus. Environmental metallo-beta-lactamases exhibit high enzymatic activity under zinc deprivation
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE MASSIF-3 |
Synchrotron site | ESRF |
Beamline | MASSIF-3 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2018-10-22 |
Detector | DECTRIS EIGER X 4M |
Wavelength(s) | 0.9677 |
Spacegroup name | P 65 |
Unit cell lengths | 144.684, 144.684, 53.306 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 24.530 - 2.170 |
R-factor | 0.219 |
Rwork | 0.217 |
R-free | 0.25260 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1znb |
RMSD bond length | 0.014 |
RMSD bond angle | 1.301 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | PHENIX (1.14_3260) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 25.000 | 2.240 |
High resolution limit [Å] | 2.170 | 2.170 |
Rmerge | 0.058 | 0.052 |
Rpim | 0.039 | 0.754 |
Number of reflections | 33621 | 2941 |
<I/σ(I)> | 11 | |
Completeness [%] | 99.7 | 99.8 |
Redundancy | 3.5 | |
CC(1/2) | 0.998 | 0.354 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 277 | 32-36% PEG4000, 0.2 ammonium sulphate |