6S0A
Crystal Structure of Properdin (TSR domains N12 & 456)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID29 |
Synchrotron site | ESRF |
Beamline | ID29 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2016-12-12 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.9763 |
Spacegroup name | I 4 2 2 |
Unit cell lengths | 114.753, 114.753, 232.260 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 102.881 - 2.520 |
R-factor | 0.2489 |
Rwork | 0.248 |
R-free | 0.26720 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.008 |
RMSD bond angle | 1.731 |
Data reduction software | DIALS |
Data scaling software | STARANISO |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0238) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 102.881 | 2.709 |
High resolution limit [Å] | 2.516 | 2.516 |
Rmerge | 0.185 | 1.639 |
Rmeas | 0.196 | 1.722 |
Rpim | 0.063 | 0.522 |
Number of reflections | 16212 | 810 |
<I/σ(I)> | 7.5 | 1.5 |
Completeness [%] | 60.5 | 15.5 |
Redundancy | 8.8 | 10.8 |
CC(1/2) | 0.996 | 0.629 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 5.5 | 291 | Sodium Citrate, PEG 3000 |