6R6Q
HIV capsid hexamer with IP5 ligand
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | DIAMOND BEAMLINE I03 |
| Synchrotron site | Diamond |
| Beamline | I03 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2019-03-03 |
| Detector | OXFORD SAPPHIRE CCD |
| Wavelength(s) | 0.978 |
| Spacegroup name | P 6 |
| Unit cell lengths | 90.693, 90.693, 56.958 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 78.000 - 2.730 |
| R-factor | 0.22401 |
| Rwork | 0.221 |
| R-free | 0.28881 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 6es8 |
| RMSD bond length | 0.006 |
| RMSD bond angle | 1.445 |
| Data reduction software | Adxv |
| Data scaling software | Aimless |
| Phasing software | PHASER |
| Refinement software | REFMAC (5.8.0238) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 78.000 | 2.790 |
| High resolution limit [Å] | 2.730 | 2.730 |
| Rmerge | 0.140 | 0.582 |
| Number of reflections | 7234 | 956 |
| <I/σ(I)> | 6.5 | |
| Completeness [%] | 92.9 | 91 |
| Redundancy | 6.9 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | BATCH MODE | 293 | PEG 6K, 0.1M NaCl |
