Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SOLEIL BEAMLINE PROXIMA 2 |
| Synchrotron site | SOLEIL |
| Beamline | PROXIMA 2 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2017-09-20 |
| Detector | DECTRIS EIGER X 9M |
| Wavelength(s) | 0.980097 |
| Spacegroup name | C 2 2 2 |
| Unit cell lengths | 69.550, 93.640, 62.230 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 19.450 - 1.900 |
| R-factor | 0.232 |
| Rwork | 0.231 |
| R-free | 0.25100 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.008 |
| RMSD bond angle | 1.130 |
| Data reduction software | XDS |
| Phasing software | PHASER |
| Refinement software | BUSTER (2.10.3) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 47.000 | |
| High resolution limit [Å] | 1.900 | 1.900 |
| Rmerge | 0.177 | |
| Rmeas | 0.199 | |
| Rpim | 0.078 | |
| Number of reflections | 16308 | |
| <I/σ(I)> | 6.6 | |
| Completeness [%] | 99.7 | |
| Redundancy | 6 | |
| CC(1/2) | 0.990 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 5.5 | 293 | 1.05 M A.S 0.06 M sodium citrate, pH 5.5 with 35 mM NaSCN. |
