6QY7
Human CSNK2A1 bound to ERB-041
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | DIAMOND BEAMLINE I03 |
| Synchrotron site | Diamond |
| Beamline | I03 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2015-09-13 |
| Detector | DECTRIS PILATUS 2M |
| Wavelength(s) | 0.97625 |
| Spacegroup name | P 43 21 2 |
| Unit cell lengths | 126.938, 126.938, 127.089 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 89.810 - 2.100 |
| R-factor | 0.19807 |
| Rwork | 0.196 |
| R-free | 0.23538 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 3pe1 |
| RMSD bond length | 0.008 |
| RMSD bond angle | 1.220 |
| Data reduction software | MOSFLM |
| Data scaling software | Aimless |
| Phasing software | PHASER |
| Refinement software | REFMAC (5.8.0230) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 89.810 | 2.150 |
| High resolution limit [Å] | 2.100 | 2.100 |
| Rmerge | 0.070 | 0.980 |
| Number of reflections | 61130 | 4476 |
| <I/σ(I)> | 14.4 | 1.9 |
| Completeness [%] | 100.0 | 100 |
| Redundancy | 8 | 7 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 7.5 | 277 | 10% PEG6000, 2M sodium chloride |
