6QW3
Calcium-bound gelsolin domain 2
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I04 |
Synchrotron site | Diamond |
Beamline | I04 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2019-02-10 |
Detector | DECTRIS EIGER X 16M |
Wavelength(s) | 0.9795 |
Spacegroup name | P 2 21 21 |
Unit cell lengths | 26.653, 50.275, 70.819 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 40.995 - 1.300 |
R-factor | 0.1556 |
Rwork | 0.154 |
R-free | 0.17390 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1kcq |
RMSD bond length | 0.016 |
RMSD bond angle | 1.469 |
Data reduction software | DIALS |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | PHENIX ((1.10.1_2155: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 70.820 | 1.320 |
High resolution limit [Å] | 1.300 | 1.300 |
Rmerge | 0.077 | 0.764 |
Rmeas | 0.080 | 0.874 |
Rpim | 0.023 | 0.409 |
Number of reflections | 24096 | 1103 |
<I/σ(I)> | 14 | 1.8 |
Completeness [%] | 99.5 | 92.9 |
Redundancy | 10.8 | 4.3 |
CC(1/2) | 0.999 | 0.579 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 5.5 | 298 | 36% PEG5000 MME, 0.1M Sodium Acetate |