6QV7

Crystal structure of a CHAD domain from Chlorobium tepidum

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SLS BEAMLINE X06DA
Synchrotron site	SLS
Beamline	X06DA
Temperature [K]	100
Detector technology	PIXEL
Collection date	2018-11-26
Detector	DECTRIS PILATUS 2M
Wavelength(s)	0.977948
Spacegroup name	I 2 2 2
Unit cell lengths	69.483, 95.735, 102.779
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	36.805 - 1.720
R-factor	0.1903
Rwork	0.189
R-free	0.22180
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	3e0s
RMSD bond length	0.010
RMSD bond angle	1.071
Data reduction software	XDS
Data scaling software	XDS
Phasing software	PHASER
Refinement software	PHENIX ((1.14_3260: ???))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	36.805	1.820
High resolution limit [Å]	1.720	1.720
Rmeas	0.074	2.210
Number of reflections	70380	11411
<I/σ(I)>	16.1	1
Completeness [%]	100.0	99.8
Redundancy	7	7.1
CC(1/2)	1.000	0.500

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP		298	2 M (NH4)2SO4, 5 % isopropanol