6QUH
GHK tagged GFP variant crystal form II at 1.34A wavelength
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PETRA III, DESY BEAMLINE P11 |
Synchrotron site | PETRA III, DESY |
Beamline | P11 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2018-05-24 |
Detector | DECTRIS PILATUS3 6M |
Wavelength(s) | 1.34 |
Spacegroup name | P 2 21 21 |
Unit cell lengths | 53.476, 99.307, 102.011 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 71.160 - 1.500 |
R-factor | 0.1442 |
Rwork | 0.142 |
R-free | 0.18750 |
Structure solution method | SAD |
RMSD bond length | 0.007 |
RMSD bond angle | 1.407 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | CRANK2 |
Refinement software | REFMAC (5.8.0253) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 99.310 | 1.530 |
High resolution limit [Å] | 1.500 | 1.500 |
Rpim | 0.044 | 0.524 |
Number of reflections | 87711 | 8625 |
<I/σ(I)> | 12.1 | |
Completeness [%] | 100.0 | |
Redundancy | 12.3 | |
CC(1/2) | 0.992 | 0.468 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 293 | 0.1M Sosium Acetate pH 5.4, 30%MPD, 0.1M Cacl2 |