6QPK

Zt-KP6-1: an effector from Zymoseptoria tritici

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	ESRF BEAMLINE MASSIF-1
Synchrotron site	ESRF
Beamline	MASSIF-1
Temperature [K]	270
Detector technology	PIXEL
Collection date	2018-04-19
Detector	DECTRIS PILATUS3 2M
Wavelength(s)	0.966
Spacegroup name	P 21 21 21
Unit cell lengths	39.395, 57.294, 79.355
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	46.450 - 1.360
R-factor	0.14
Rwork	0.140
R-free	0.18000
Structure solution method	SAD
Data reduction software	XDS
Data scaling software	Aimless (0.6.3)
Phasing software	HKL2Map
Refinement software	REFMAC (5.8.0222)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	46.450	1.400
High resolution limit [Å]	1.360	1.360
Rmerge	0.051
Number of reflections	448165	5272
<I/σ(I)>	18.7	2.5
Completeness [%]	91.3	56.7
Redundancy	6.01	10.4
CC(1/2)		0.450

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	EVAPORATION		298	0,1M Tris pH 9, 1.5M LiSO4