6QNR
70S ribosome elongation complex (EC) with experimentally assigned potassium ions
This is a non-PDB format compatible entry.
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06SA |
Synchrotron site | SLS |
Beamline | X06SA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2008-11-10 |
Detector | PSI PILATUS 6M |
Wavelength(s) | 1.000 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 209.460, 446.200, 623.050 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 223.100 - 3.100 |
R-factor | 0.1981 |
Rwork | 0.196 |
R-free | 0.25320 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4v6f |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | PHENIX (1.13_2998) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 223.100 | 6.000 | 3.200 |
High resolution limit [Å] | 3.100 | 5.850 | 3.100 |
Rmerge | 0.600 | ||
Number of reflections | 1043872 | 22459 | 94202 |
<I/σ(I)> | 6.94 | 1 | 1.9 |
Completeness [%] | 96.5 | 99.6 | 88.4 |
Redundancy | 9.1 | 8.86 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.5 | 293 | Tris-OAc, KSCN, PEG-20k, PEG-550mme |
1 | VAPOR DIFFUSION, HANGING DROP | 7.5 | 293 | Tris-OAc, KSCN, PEG-20k, PEG-550mme |
1 | VAPOR DIFFUSION, HANGING DROP | 7.5 | 293 | Tris-OAc, KSCN, PEG-20k, PEG-550mme |
1 | VAPOR DIFFUSION, HANGING DROP | 7.5 | 293 | Tris-OAc, KSCN, PEG-20k, PEG-550mme |
1 | VAPOR DIFFUSION, HANGING DROP | 7.5 | 293 | Tris-OAc, KSCN, PEG-20k, PEG-550mme |
1 | VAPOR DIFFUSION, HANGING DROP | 7.5 | 293 | Tris-OAc, KSCN, PEG-20k, PEG-550mme |
1 | VAPOR DIFFUSION, HANGING DROP | 7.5 | 293 | Tris-OAc, KSCN, PEG-20k, PEG-550mme |
1 | VAPOR DIFFUSION, HANGING DROP | 7.5 | 293 | Tris-OAc, KSCN, PEG-20k, PEG-550mme |