Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ALBA BEAMLINE XALOC |
| Synchrotron site | ALBA |
| Beamline | XALOC |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2015-02-08 |
| Detector | DECTRIS PILATUS3 6M |
| Wavelength(s) | 0.9793 |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 80.209, 46.265, 87.987 |
| Unit cell angles | 90.00, 115.06, 90.00 |
Refinement procedure
| Resolution | 39.850 - 1.660 |
| R-factor | 0.1708 |
| Rwork | 0.169 |
| R-free | 0.19950 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 2a0k |
| RMSD bond length | 0.008 |
| RMSD bond angle | 0.895 |
| Data reduction software | XDS |
| Data scaling software | XDS |
| Phasing software | PHASER |
| Refinement software | PHENIX ((1.14_3260: ???)) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 39.850 | 1.700 |
| High resolution limit [Å] | 1.660 | 1.660 |
| Rmeas | 0.052 | |
| Rpim | 0.028 | |
| Number of reflections | 33859 | |
| <I/σ(I)> | 18.3 | |
| Completeness [%] | 97.7 | |
| Redundancy | 6.8 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 291 | 25% PEG 3350, 0.2 M magnesium chloride, 0.1 M Tris-HCl, pH 8.5 |
