6PRM
Crystal structure of apo PsS1_19B
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | CLSI BEAMLINE 08ID-1 |
Synchrotron site | CLSI |
Beamline | 08ID-1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2013-12-05 |
Detector | RAYONIX MX-300 |
Wavelength(s) | 0.97949 |
Spacegroup name | P 1 |
Unit cell lengths | 48.510, 88.580, 106.600 |
Unit cell angles | 82.22, 79.85, 84.20 |
Refinement procedure
Resolution | 47.600 - 2.500 |
R-factor | 0.2393 |
Rwork | 0.238 |
R-free | 0.27310 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 6bia |
RMSD bond length | 0.007 |
RMSD bond angle | 1.426 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0238) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 104.200 | 2.570 |
High resolution limit [Å] | 2.500 | 2.500 |
Rmerge | 0.108 | 0.334 |
Number of reflections | 58432 | 4508 |
<I/σ(I)> | 8.4 | |
Completeness [%] | 97.9 | |
Redundancy | 3.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 291 | PEG 3350, sodium acetate trihydrate |