6PGF
WDR5delta32 bound to N-(4-(4-(hydroxymethyl)-1H-imidazol-2-yl)butyl)acrylamide
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | AUSTRALIAN SYNCHROTRON BEAMLINE MX2 |
Synchrotron site | Australian Synchrotron |
Beamline | MX2 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2017-05-02 |
Detector | DECTRIS EIGER X 16M |
Wavelength(s) | 0.95373 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 46.819, 65.127, 97.422 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 48.710 - 1.540 |
R-factor | 0.14917 |
Rwork | 0.148 |
R-free | 0.16952 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 6pg4 |
RMSD bond length | 0.008 |
RMSD bond angle | 1.411 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0238) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 48.710 | 1.570 |
High resolution limit [Å] | 1.540 | 1.540 |
Number of reflections | 43339 | 1913 |
<I/σ(I)> | 16.2 | 3.2 |
Completeness [%] | 97.1 | 88 |
Redundancy | 13.3 | 12 |
CC(1/2) | 0.999 | 0.847 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 281 | 0.16 M ammonium sulfate, 0.1 M Bis-Tris chloride, pH 6.1, 30.1% w/v PEG8000 |