6OOM

PROTEIN A

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	APS BEAMLINE 23-ID-B
Synchrotron site	APS
Beamline	23-ID-B
Temperature [K]	100
Detector technology	CCD
Collection date	2017-10-10
Detector	MAR CCD 130 mm
Wavelength(s)	1
Spacegroup name	C 1 2 1
Unit cell lengths	95.239, 63.031, 102.340
Unit cell angles	90.00, 101.28, 90.00

Refinement procedure

Resolution	15.000 - 2.200
Structure solution method	SAD
Data reduction software	HKL-2000
Data scaling software	HKL-2000
Phasing software	SHARP
Refinement software	REFMAC

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	15.000	2.300
High resolution limit [Å]	2.200	2.200
Number of reflections	26746	300
<I/σ(I)>	10
Completeness [%]	93.0
Redundancy	3

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP	6	293	PEG 400, magnesium chloride