6OKM

Human OX40R (TNFRSF4) bound to Fab 3C8

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	ALS BEAMLINE 5.0.2
Synchrotron site	ALS
Beamline	5.0.2
Temperature [K]	100
Detector technology	PIXEL
Collection date	2016-05-04
Detector	DECTRIS PILATUS3 6M
Wavelength(s)	1.00000
Spacegroup name	P 41 2 2
Unit cell lengths	117.006, 117.006, 118.907
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	47.890 - 2.100
R-factor	0.212
Rwork	0.211
R-free	0.23800
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.010
RMSD bond angle	1.150
Data reduction software	HKL-2000
Data scaling software	HKL-2000
Phasing software	PHASER
Refinement software	BUSTER (2.11.6)

Data quality characteristics

	Overall	Inner shell	Outer shell
Low resolution limit [Å]	50.000	50.000	2.180
High resolution limit [Å]	2.100	4.520	2.100
Rmerge	0.076	0.040	0.694
Rmeas	0.079	0.042	0.735
Rpim	0.022	0.012	0.236
Total number of observations	611148
Number of reflections	48817	5201	4754
<I/σ(I)>	5.9
Completeness [%]	99.9	100	99.3
Redundancy	12.5	12.3	9
CC(1/2)		0.999	0.881

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, SITTING DROP		293