6OID

Redox Regulation of FN3K from Arabidopsis thaliana

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	APS BEAMLINE 22-ID
Synchrotron site	APS
Beamline	22-ID
Temperature [K]	100
Detector technology	CCD
Collection date	2017-11-30
Detector	MARRESEARCH
Wavelength(s)	1.0
Spacegroup name	C 2 2 21
Unit cell lengths	158.860, 163.640, 70.720
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	53.504 - 2.365
R-factor	0.1765
Rwork	0.175
R-free	0.20400
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	3f7w 3jr1 and 5IGS
RMSD bond length	0.009
RMSD bond angle	1.071
Data reduction software	XDS
Data scaling software	XSCALE
Phasing software	PHASER
Refinement software	PHENIX ((1.12_2829: ???))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	53.504	2.430
High resolution limit [Å]	2.350	2.370
Rmeas	0.157
Number of reflections	38000	2683
<I/σ(I)>	14.3
Completeness [%]	99.8	97.1
Redundancy	14.5	14.6
CC(1/2)	0.999	0.520

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP	5.5	298	2 M Ammonium sulfate, 0.1 M MES pH 5.5