6OHT

Structure of EBP and U18666A

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	APS BEAMLINE 19-ID
Synchrotron site	APS
Beamline	19-ID
Temperature [K]	100
Detector technology	PIXEL
Collection date	2018-11-16
Detector	DECTRIS PILATUS 6M
Wavelength(s)	0.979
Spacegroup name	P 21 21 2
Unit cell lengths	194.566, 67.823, 96.858
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	48.642 - 3.200
R-factor	0.2735
Rwork	0.269
R-free	0.31910
Structure solution method	SAD
RMSD bond length	0.004
RMSD bond angle	0.927
Data reduction software	HKL-3000
Data scaling software	HKL-3000
Phasing software	PHENIX
Refinement software	PHENIX ((1.12_2829: ???))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	50.000	3.260
High resolution limit [Å]	3.200	3.138
Number of reflections	28389	2273
<I/σ(I)>	30
Completeness [%]	99.8
Redundancy	12.9
CC(1/2)	0.990	0.739

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP		293.15	Hepes, peg 600