6O5K
Murine TRIM28 Bbox1 domain
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | AUSTRALIAN SYNCHROTRON BEAMLINE MX1 |
Synchrotron site | Australian Synchrotron |
Beamline | MX1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2015-12-12 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 0.9537 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 33.012, 51.459, 72.884 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 42.040 - 1.600 |
R-factor | 0.18181 |
Rwork | 0.180 |
R-free | 0.20764 |
Structure solution method | SAD |
RMSD bond length | 0.007 |
RMSD bond angle | 1.194 |
Data reduction software | XDS (Jan 10, 2014) |
Data scaling software | Aimless |
Phasing software | SHELXCD |
Refinement software | REFMAC (5.8.0230) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 42.040 | 1.630 |
High resolution limit [Å] | 1.600 | 1.600 |
Rmerge | 0.267 | 3.950 |
Rpim | 0.072 | 1.075 |
Number of reflections | 17060 | 817 |
<I/σ(I)> | 10.3 | 0.97 |
Completeness [%] | 100.0 | 100 |
Redundancy | 14.3 | 14.2 |
CC(1/2) | 0.997 | 0.391 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 6 | 291 | 2.7 M Ammonium sulfate, pH 6.0 |