6O2E
GCN4 with asparagine at position 18
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | ENRAF-NONIUS FR591 |
Temperature [K] | 293 |
Detector technology | CCD |
Collection date | 2018-03-29 |
Detector | APEX II CCD |
Wavelength(s) | 1.5406 |
Spacegroup name | I 21 21 21 |
Unit cell lengths | 19.251, 30.016, 107.053 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 53.526 - 1.896 |
R-factor | 0.2179 |
Rwork | 0.214 |
R-free | 0.24740 |
Data reduction software | PROTEUM PLUS |
Data scaling software | PROTEUM PLUS |
Phasing software | PHENIX |
Refinement software | PHENIX (1.13_2998) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 53.526 |
High resolution limit [Å] | 1.896 |
Number of reflections | 4721 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 293 | Pact premier C1 |