6NZ5

YcjX-GDPCP

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	APS BEAMLINE 19-ID
Synchrotron site	APS
Beamline	19-ID
Temperature [K]	100
Detector technology	PIXEL
Collection date	2018-10-26
Detector	DECTRIS PILATUS 6M
Wavelength(s)	0.9794
Spacegroup name	P 21 21 21
Unit cell lengths	59.471, 128.257, 148.056
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	46.363 - 2.233
R-factor	0.1798
Rwork	0.178
R-free	0.21700
RMSD bond length	0.003
RMSD bond angle	0.577
Data reduction software	HKL-3000
Data scaling software	HKL-3000
Phasing software	PHENIX
Refinement software	PHENIX ((1.14_3260: ???))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	50.000	2.260
High resolution limit [Å]	2.220	2.220
Number of reflections	54859
<I/σ(I)>	19
Completeness [%]	98.6
Redundancy	6.4

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP	6.5	287	100 mM HEPES pH 6.5 and 6% (w/v) polyvinyl pyrrolidone