6NOY
Structure of Cyanothece McdB
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ALS BEAMLINE 8.3.1 |
Synchrotron site | ALS |
Beamline | 8.3.1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2018-12-19 |
Detector | DECTRIS PILATUS3 6M |
Wavelength(s) | 0.979 |
Spacegroup name | P 32 2 1 |
Unit cell lengths | 95.500, 95.500, 177.100 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 74.937 - 3.460 |
R-factor | 0.2301 |
Rwork | 0.226 |
R-free | 0.27160 |
Structure solution method | SAD |
RMSD bond length | 0.004 |
RMSD bond angle | 0.745 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | AutoSol |
Refinement software | PHENIX (1.12_2829) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 75.000 | 3.650 |
High resolution limit [Å] | 3.460 | 3.460 |
Rpim | 0.047 | 0.653 |
Number of reflections | 23328 | |
<I/σ(I)> | 16.5 | 1.9 |
Completeness [%] | 99.1 | 98.6 |
Redundancy | 8.5 | 8.8 |
CC(1/2) | 0.999 | 0.776 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 298 | 1.5 M ammonium sulfate, 0.1 M sodium acetate |